Author supplied from the article: Abstract A temperature compensated hydrogen sensor was designed and made capable of detecting H2 within a broad range of 100–10.000 ppm while compensating instantaneously for large (±25 °C) temperature variations. Two related operational constraints have been simultaneously addressed: (1) Selective, and sensitive detection under large temperature changes, (2) Fast warning at low and increasing H2 levels. Accurate measurements of hydrogen concentrations were enabled by matching relevant time-constants. This was achieved with a microchip having two temperature coupled palladium nanowires. One of the H2 sensitive Pd nanowires was directly exposed to hydrogen, whilst the other nanowire was used as a temperature sensor and as a reference. A drop forging technique was used to passivate the second Pd wire against H2 sensing. Temperature effects could be substantially reduced with a digital signal processing algorithm. Measurements were done in a test chamber, enabling the hydrogen concentration to be controlled over short and long periods. An early response for H2 sensing is attainable in the order of 600 milliseconds and an accurate value for the absolute hydrogen concentration can be obtained within 15 s.
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From the article: "A facile approach for the fabrication of large-scale interdigitated nanogap electrodes (nanogap IDEs) with a controllable gap was demonstrated with conventional micro-fabrication technology to develop chemocapacitors for gas sensing applications. In this work, interdigitated nanogap electrodes (nanogap IDEs) with gaps from 50–250 nm have been designed and processed at full wafer-scale. These nanogap IDEs were then coated with poly(4-vinyl phenol) as a sensitive layer to form gas sensors for acetone detection at low concentrations. These acetone sensors showed excellent sensing performance with a dynamic range from 1000 ppm to 10 ppm of acetone at room temperature and the observed results are compared with conventional interdigitated microelectrodes according to our previous work. Sensitivity and reproducibility of devices are discussed in detail. Our approach of fabrication of nanogap IDEs together with a simple coating method to apply the sensing layer opens up possibilities to create various nanogap devices in a cost-effective manner for gas sensing applications"
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From Springer description: "We present the design considerations of an autonomous wireless sensor and discuss the fabrication and testing of the various components including the energy harvester, the active sensing devices and the power management and sensor interface circuits. A common materials platform, namely, nanowires, enables us to fabricate state-of-the-art components at reduced volume and show chemical sensing within the available energy budget. We demonstrate a photovoltaic mini-module made of silicon nanowire solar cells, each of 0.5 mm2 area, which delivers a power of 260 μW and an open circuit voltage of 2 V at one sun illumination. Using nanowire platforms two sensing applications are presented. Combining functionalised suspended Si nanowires with a novel microfluidic fluid delivery system, fully integrated microfluidic–sensor devices are examined as sensors for streptavidin and pH, whereas, using a microchip modified with Pd nanowires provides a power efficient and fast early hydrogen gas detection method. Finally, an ultra-low power, efficient solar energy harvesting and sensing microsystem augmented with a 6 mAh rechargeable battery allows for less than 20 μW power consumption and 425 h sensor operation even without energy harvesting."
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